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Details
Inventors: Bishop, Alan W.; Bray, David J.; Gardiner, Robert W.; Viney, Brian W.;
Assignee: The Secretary of the State for Defence in Her Britannic Majesty's (Hants, GB2)
Primary Examiner: Rosenberg; Peter D.
Assistant Examiner:
Attorney, Agent or Firm: Nixon & Vanderhye

Apparatus for the physical vapor deposition of an alloy whose constituent ements have widely differing vapor pressures comprises an inner evaporation crucible (1) surrounded by a second evaporation crucible (2) having an array of nozzles (9) angled towards collector (5). In use of the apparatus, a charge (3) of relatively low volatility is evaporated from inner crucible (1) using an electron beam (7) focussed by magnet (8). Charge (4) in second crucible (2) is of much higher volatility and is evaporated by radiant heating. The nozzles (9) direct the vapor from charge (4) along pathways which intersect the vapor rising from charge (3) such that the combined vapor stream reaching collector (5) is an intimate mixture of constituents. The nozzles (9) may also serve to control the flow rate of vapor from the second crucible (2).

DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS Referring now to FIG.
1, there is shown an inner evaporation crucible 1 surrounded by a second evaporation crucible 2.
The inner evaporation crucible 1 contains a charge 3 of a relatively low volatility constituent whilst second evaporation crucible 2 is charged with a much higher volatility constituent 4, such as magnesium.
The crucibles are centrally positioned under a collector 5 on which a deposit 6 is accumulated.
In use of the apparatus, the charge 3 in the inner evaporation crucible 1 is heated using an electron beam 7 focussed by magnet 8 to a temperature which causes a stream of vapour to rise towards collector 5.
Second evaporation crucible 2 is heated by radiant heaters (not shown) to generate an appreciable vapour pressure in the magnesium 4, such that streams of magnesium vapour are discharged towards the collector 5 through nozzles 9.
The nozzles 9 are angled towards the collector 5 so that the streams of magnesium vapour intersect the stream of vapour rising from the inner evaporation crucible 1.
This ensures that the combined vapour impinging on the collector 5 is an intimate mixture of constituents.
Each stream of magnesium vapour diverges after it leaves its respective nozzle 9 so the spacing between individual nozzles and their separation from the collector 5 is arranged such that a uniform population of magnesium atoms is delivered to the collector across a large proportion of its total surface area.
The separation between the inner evaporation crucible 1 and the collector 5 is also chosen to give uniform coverage over as much of the collector as possible.
FIGS.
2 and 3 show a preferred form of the apparatus in plan view and sectional view, respectively.
Here the inner evaporation crucible 10 is shown as a water-cooled copper crucible which is surrounded by an annular steel crucible 20.
Annular steel crucible 20 is covered with a steel lid 21 having eight nozzles 40 disposed around its inner circumference, which nozzles are convergently directed towards a collector (not shown) positioned above the inner crucible 10



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